Chapter 9

Solid Samples

Important Topics

Sampling concerns
Sample preparation
Dry and wet samples
pH measurements
Metals in soils and sediments
Organics in solids
volatiles by purge and trap or headspace
solid phase microextraction
Semivolatiles
Sample cleanup
TCLP
Immunoassay

Important Skills

Selection of proper sample preparation and analytical method for a particular sample and analyte
Calculations of analyte concentration on dry basis from wet sample data
Methods of sample validation
Calculation of concentrations from calibration and experimental data

Homework solutions

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