Synthesis and Characterization of High Temperature Superconductors
Week 1
Literature Search On High Temperature Superconductors (Background)
(WWW, Electronic Journals and Library)
Write 10 Page Summary
Week 2
Structure, Chemical Composition and Preparation of Bulk Superconductor
- Yttrium Barium Copper Oxide (YBa2Cu3O6+x,= YBCO)
(WWW, Electronic Journals and Library)
Write down, in your own words, a detailed procedure for preparing YBCO by solid phase reaction
Week 3
Structure, Chemical Composition and Preparation of Bulk Superconductor
- Yttrium Barium Copper Oxide (YBa2Cu3O6+x,= YBCO)
(WWW, Electronic Journals and Library)
Week 4
Structure, Chemical Composition and Preparation of Bulk Superconductor
- Yttrium Barium Copper Oxide (YBa2Cu3O6+x,= YBCO)
(WWW, Electronic Journals and Library)
Inspect YBCO sample and determine purity (look for non-uniform color)
Grind powder sample for 40 minutes and reheat (cook).
Work on methods of sample characterization
Week 5
Structure, Chemical Composition and Preparation of Bulk Superconductor
- Yttrium Barium Copper Oxide (YBa2Cu3O6+x,= YBCO)
(WWW, Electronic Journals and Library)
Carefully read C "Manual"
Type-in and execute test programs
Run programs to compute diffraction pattern of YBCO
Compare all measured diffraction peaks with those that you have computed
Week 6
Structure, Chemical Composition and Preparation of Bulk Superconductor
- Yttrium Barium Copper Oxide (YBa2Cu3O6+x,= YBCO)
(WWW, Electronic Journals and Library)
Convert Weekly Exercises into Presentation
Outline Presentation and Prepare Overheads
Outline (Suggestion)
I. Background and History
- Discovery
- History of Superconductivity
- Compare and Contrast Conventional and High Temperature Superconductors
- Physics of Superconductivity
- Technological Applications
II. Preparation of YBCO
- Stoichiometry Example
- Case for YBCO
- Details of Preparation
III. Characterization
- Crystal Structure of YBCO
- Details of X-Ray Diffraction Measurements
- Simulation of X-Ray Diffraction Pattern
- Identification of YBCO Phase
- Meissner Effect
Week 7
Structure, Chemical Composition and Preparation of Bulk Superconductor
- Yttrium Barium Copper Oxide (YBa2Cu3O6+x,= YBCO)
(WWW, Electronic Journals and Library)
Raman Scattering
Write 4 page section on Raman Scattering (or Raman Spectroscopy)
What is Raman Scattering?
What can Raman Scattering Tell You about YBCO?
Monday: Do WWW Search
Tuesday: Go to Library and Look-Up Books on Raman Scattering
Wednesday: Work on YBCO Raman measurements with Prof. Federeici
Combine all components into 15-20 Page Report